Hanna-instruments HI 98180 Manuel d'utilisateur

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Page 1 - HI 98184 HI 98185

1Calibration CheckWaterproofpH/mV/ISE/TemperatureMetersHI 98180 HI 98181HI 98182 HI 98183HI 98184 HI 98185Instruction Manualwww.hannainst.com

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10HI 98182 AND HI 98183HI 98182 AND HI 98183HI 98182 AND HI 98183HI 98182 AND HI 98183HI 98182 AND HI 98183SPECIFICATIONSSPECIFICATIONSSPECIFICATIONSS

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11EGNARHp0.02ot0.2–Hp00.2ot00.2–Hp000.2ot000.2–Vm0002±5E00.1ot3-E00.1morF(.cnoc 48189IH )01E99.9ot7-E00.1morF(.cnoc 58189IH ))Fº0.842ot0.4–(Cº0.021ot0

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12OPERATIONAL GUIDEOPERATIONAL GUIDEOPERATIONAL GUIDEOPERATIONAL GUIDEOPERATIONAL GUIDEINITIAL PREPARATIONThe instrument is supplied complete with rec

Page 5 - Front view

13Allow for the electrode to adjust and reading to stabilize (hourglass symbolturns off).On the pH screen are displayed:• pH reading with the selected

Page 6 - Top view

14ORP MEASUREMENTS (not for HI 98180)To perform ORP measurements, connect an optional ORP electrode (see “Accessories“section) to the instrument and t

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15Enter the ISE mode by pressing RANGE until the display changes to ISErange.Submerge the ISE electrode tip (4cm/1½”) into the sampleto be tested and

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16pppppH CALIBRATIONH CALIBRATIONH CALIBRATIONH CALIBRATIONH CALIBRATIONIt is recommended to calibrate the instrument frequently, especially if highac

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17• Press CAL. The instrument will display the measured pH, the LCD firstexpected buffer and the temperature reading.• If necessary, press the ARROW k

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18• When the reading is stable and close to the selected buffer, the CFMfunctional key is displayed.• Press CFM to confirm calibration.• The calibrate

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19• After the third calibration point is confirmed, immerse the pH electrodeand the temperature probe approximately 4 cm (1½”) into the fourthbuffer s

Page 12 - OPERATIONAL GUIDE

2WARRANTYWARRANTYWARRANTYWARRANTYWARRANTYDear Customer,Thank you for choosing a Hanna Instruments product.Please read this instruction manual carefull

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20• Press CFM to confirm calibration.• The instrument stores the calibration values and returns to normal mea-surement mode.FOUR, THREE or TWO-POINT C

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21ERROR SCREENSWrong bufferThe calibration cannot be confirmed.The pH reading is not close to the selected buffer. Select another buffer usingthe ARRO

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22Wrong old slopeAn inconsistency between new and previous (old) calibration is detected. Clearold calibration parameters and proceed calibration from

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23WORKING WITH CUSTOM BUFFERSIf at least one custom buffer was set in SETUP menu, it can be selected forcalibration by pressing the ARROW keys. The Cu

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24CLEAR CALIBRATIONPress Clear functional key when displayed or CLR key (HI 98180 &HI 98181) to clear old calibrations.All old calibrations, are c

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25The temperature has an effect on pH. The calibration buffer solutions areaffected by temperature changes to a lesser degree than normal solutions.Du

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26• Press CAL when the instrument is in RELATIVE mV measurement mode.The relative mV value and the temperature values are displayed.• Use the ARROW ke

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27It is recommended to calibrate the instrument frequently, especially if highaccuracy is required.The ISE range should be recalibrated:• Whenever the

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28• Press CAL. The primary LCD will displays the ion concentration in the selectedunit or “---” if not calibrated and first standard value.• If necess

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29• Press CFM to confirm calibration.• The calibrated value and the fourth expected standard value will bedisplayed.• After the third calibration poin

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3PRELIMINARY EXAMINATIONPRELIMINARY EXAMINATIONPRELIMINARY EXAMINATIONPRELIMINARY EXAMINATIONPRELIMINARY EXAMINATIONThe HI 9818x instruments are state

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30Wrong slopeThe calibration cannot be confirmed.This message is displayed if slope is out of the accepted range.Slope under accepted value (30 % defa

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31GOOD LABORATORY PRACTICE (GLP)GOOD LABORATORY PRACTICE (GLP)GOOD LABORATORY PRACTICE (GLP)GOOD LABORATORY PRACTICE (GLP)GOOD LABORATORY PRACTICE (GL

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32LAST RELATIVE mV CALIBRATION DATALast Relative mV calibration data is stored automatically after a successfulcalibration.To view the Relative mV cal

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33SETUPSETUPSETUPSETUPSETUPSetup mode allows viewing and modifying the measurement parameters.These are general SETUP parameters for all the ranges an

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34The following table lists the specific range parameters.Item Description Valid value DefaultCalibr. N

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35GENERAL PARAMETER SCREENSBacklightFocus on the Backlight item.Press Modify.Use / keys to change the intensity then press Accept to confirm.Press E

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36Auto Light OffFocus on the Auto Light Off item.Press 5, 10 or 30 to change settings.Auto Power OffFocus on the Auto Power Off item.Press Modify.Pres

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37Press Modify.Use / keys to select item.Use ARROW keys to change focused values.Press Accept to confirm new setting, or ESC to leave without changi

Page 32 - LAST ISE CALIBRATION DATA

38LanguageFocus on the Language item.Use the desired functional key to change the option. Wait until new languageis loaded. If language load fails the

Page 33 - SETUPSETUP

39Instrument IDFocus on the Instrument ID item.Press Modify.Use ARROW keys to change the instrument ID.Press Accept to confirm or ESC to exit without

Page 34 - Replace

4(–4 to 248 ºF), using HI 7662 interchangeable temperature probes ortemperature sensor inside pH electrode.These instruments can also measure with ORP

Page 35 - Contrast

40Meter informationFocus on the Meter Information item.Press Select.The meter informations are displayed:-firmware version-language version-mV and tem

Page 36 - Date/Time

41Note: If enabled “CAL DUE” warning will be displayed, the set number ofdays after calibration is over passed.First point modeFocus on the First Poin

Page 37 - Date Format

42Press Modify to set custom buffer value.Use ARROW keys to change the value.Press Accept to confirm custom buffer value or ESC to exit without saving

Page 38 - Temperature

43ISE probeFocus on the ISE probe item.Press Custom in order to set the parameters for a custom probe.Press Standard in order to select one probe from

Page 39 - Baud Rate

44Focus on Molar Weight.Press Modify in order to change molar weight.Use ARROW keys to change the value. Press Accept to confirm or ESC to exit.If Sta

Page 40 - Calibration Timeout

45Press Modify.Use ARROW key to select unit.Press Accept to confirm selection or ESC to exit.Note:• If the unit is changed or “User” is selected a war

Page 41 - Custom Buffers

46This feature allows the user to log pH, Rel mV or ISE measurements. All loggeddata can be transferred to a PC through the USB (RS232) port.The maxim

Page 42 - Out of Cal-Range Warning

47If More is pressed.Use ARROW keys to scroll between complete log information.If Delete is pressed.Use ARROW key to focus the record to be deleted an

Page 43 - Change Slope

48AAAAAutoEndutoEndutoEndutoEndutoEndTo freeze the first stable reading on the LCD press AutoEnd while the instru-ment is in measurement mode.The ”Wai

Page 44 - ISE unit

49mmmmmV V V V V andandandandand TEMPERATURE CALIBRATION TEMPERATURE CALIBRATION TEMPERATURE CALIBRATION TEMPERATURE CALIBRATION TEMPERATURE CALIBRATI

Page 45

51) Liquid Crystal Display (LCD).2) Functional keys.3) / keys to manually increase/decrease the parameters or to scroll betweenthe parameter list.4)

Page 46 - LOGGINGLOGGING

50• Press CFM to confirm.• The second expected calibrated point is displayed.• Immerse the temperature probe into the second vessel as close as possib

Page 47

51displayed.• Set 1800.0 mV on the simulator.• When the reading is stable and close to the selected calibration point, theCFM functional key is displa

Page 48

52PC INTERFACEPC INTERFACEPC INTERFACEPC INTERFACEPC INTERFACE(((((not fornot fornot fornot fornot for HI 98180, HI 98181) HI 98180, HI 98181) HI 9818

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53OFF Is equivalent to pressing OFF keyCHR xx Change the instrument range according with the parametervalue (xx):• xx=00 pH range/0.001 resolution• xx

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54• 05 - ISE range• Meter status (2 chars of status byte): represents a 8 bithexadecimal encoding.• 0x10 - temperature probe is connected• 0x01 - new

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55• buffer value, with sign and decimal point and expo-nent (11 chars).• calibration time, yymmddhhmmss (12 chars).• electrode condition, with sign (3

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56• The ion charge (2 chars)• The ISE unit (2 chars)• The short name of the selected language (3 chars)NSLx Requests the number of logged samples (4 c

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57Notes: • “Err8” is sent if the instrument is not in measurement mode.• “Err6” is sent if the requested range is not available.• “Err4” is sent if th

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58The instrument is ready with rechargeable batteries inside.First time you start working with the instrument or when the rechargeablebatteries are ch

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59To recharge the rechargeable batteries, follow the next steps:• Connect the 12VDC power adapter to the main line and to the main line of thebattery

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614) BNC electrode connector.15) Temperature socket.Top viewTop viewTop viewTop viewTop view

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60The resistance of glass electrodes partially depends on the temperature. The lowerthe temperature, the higher the resistance. It takes more time for

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61PREPARATION PROCEDURERemove the electrode protective cap.DO NOT BE ALARMED IF ANY SALT DEPOSITS ARE PRESENT. This is normalwith electrodes and they

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62For refillable electrodes:For refillable electrodes:For refillable electrodes:For refillable electrodes:For refillable electrodes:If the filling sol

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63Follow the Storage Procedure above.pH CLEANING PROCEDURE• GeneralSoak in Hanna HI 7061 or HI 8061 GeneralCleaning Solution for approximately ½ hour.

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64TROUBLESHOOTING GUIDETROUBLESHOOTING GUIDETROUBLESHOOTING GUIDETROUBLESHOOTING GUIDETROUBLESHOOTING GUIDESMOTPMYS MELBORP NOITULOSevissecxe/esnopser

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65pH CALIBRATION SOLUTIONSHI 50004-01 pH 4.01 Buffer Solution, 20 mL sachet, 10 pcsHI 50004-02 pH 7.01 Buffer Solution, 20 mL sachet, 25 pcsHI 50007-0

Page 63 - Oil/grease

66HI 8082 3.5M KCl Electrolyte in FDA approved bottle, 4x30 mL, fordouble junction electrodesHI 8093 1M KCl+AgCl Electrolyte in FDA approved bottle, 4

Page 64 - TROUBLESHOOTING GUIDE

67HI 1131BGlass-body, single junction, refillable, combination pH electrode.Use: general purpose.HI 1330BGlass-body, semimicro, single junction, refil

Page 65 - ACCESSORIES

68HI 1332BPlastic-body (PEI), double junction, refillable, combination pH electrode.Use: general purpose.FC 100BPlastic-body (PVDF), double junction,

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69FC 911BPlastic-body (PVDF), double junction, refillable with built-in amplifier, combination pHelectrode. Use: very high humidity.HI 1413BGlass-body

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7HI 98182, HI 98183,HI 98182, HI 98183,HI 98182, HI 98183,HI 98182, HI 98183,HI 98182, HI 98183,HI 98184, AND HI 98185HI 98184, AND HI 98185HI 98184,

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70EXTENSION CABLE FOR SCREW-TYPE ELECTRODES(SCREW TO BNC ADAPTER)HI 7855/1 Extension cable 1 m (3.3') longHI 7855/3 Extension cable 3 m (9.9&ap

Page 69 - ORP ELECTRODES

71RECOMMENDATIONS FOR USERSBefore using these products, make sure they are entirely suitable for theenvironment in which they are used.Operation of th

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72SALES AND TECHNICAL SERVICE CONTACTSAustralia:Tel. (03) 9769.0666 • Fax (03) 9769.0699China:Tel. (10) 88570068 • Fax (10) 88570060Egypt:Tel. & F

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8Top viewTop viewTop viewTop viewTop view14) BNC electrode connector.15) Reference socket (HI 98184/5).16) Reference socket rubber stopper (HI 98184/5

Page 72 - MAN98185

9EGNARHp0.61ot0.2–Hp00.61ot00.2–(Vm0002± 18189IH )ylno)Fº0.842ot0.4–(Cº0.021ot0.02–NOITULOSERHp1.0Hp10.0(Vm1.0 18189IH )ylno)Fº1.0(Cº1.0YCARUCCAFº86/C

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