Hanna-instruments HI 3512 Manuel d'utilisateur

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1
Two Channels
pH/ORP/ISE,
EC/TDS/NaCl/Resistivity,
Temperature
Bench Meter
HI 3512
Instruction Manual
www.hannainst.com
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Résumé du contenu

Page 1 - Bench Meter

1Two ChannelspH/ORP/ISE,EC/TDS/NaCl/Resistivity,TemperatureBench MeterHI 3512Instruction Manualwww.hannainst.com

Page 2

10OPERATIONAL GUIDEOPERATIONAL GUIDEOPERATIONAL GUIDEOPERATIONAL GUIDEOPERATIONAL GUIDEPOWER CONNECTIONPlug the 12 Vdc adapter into the power supply s

Page 3

11Allow for the electrode to adjust and reading to stabilize (hourglasssymbol turns off).On the pH screen are displayed:• pH reading with the selected

Page 4

123 cmORP MEASUREMENTSTo perform ORP measurements, connect an ORP electrode (see ACCESSORIESsection) to the instrument and turn it ON.If necessary, en

Page 5 - FUNCTIONAL DESCRIPTION

133 cmSubmerse the ISE electrode tip 3 cm (1¼”) into thesample to be tested and wait for the reading tostabilize.The ISE reading will be displayed al

Page 6 - Rear view

14EC rangeThe conductivity range is from 0 to 400 mS/cm . The actual conductivityrange (the uncompensated conductivity) is up to 1000 mS/cm. Theinstru

Page 7 - SPECIFICATIONS

15The EC, Resistivity and TDS scales are auto-ranging. The meter automaticallysets the scale with the highest possible resolution.By pressing Lock, th

Page 8

16The conductivity of a solution with a specific electrolyte concentrationchanges with temperature. The relationship of the change in conductivityas a

Page 9

17The conductivity of an aqueous solution is the measure of its ability tocarry an electrical current by means of ionic motion.The conductivity invari

Page 10 - OPERATIONAL GUIDE

18To enter User Calibration screen press CAL key while in pH/Rel mV/ISErange (pH channel) or EC/Salinity range (EC channel).From EC rangePress the co

Page 11

19It is recommended to calibrate the instrument frequently, especially ifhigh accuracy is required.The pH range should be recalibrated:• Whenever the

Page 12

2Dear Customer,Thank you for choosing a Hanna Instruments product.Please read this instruction manual carefully before using this instrument.This manu

Page 13

20FIVE-POINT CALIBRATIONFIVE-POINT CALIBRATIONFIVE-POINT CALIBRATIONFIVE-POINT CALIBRATIONFIVE-POINT CALIBRATION• Immerse the pH electrode and the tem

Page 14

21• When the reading is stable and close to the selected buffer, theConfirm function key is displayed.• Press Confirm to confirm calibration.• The cal

Page 15 - AUTO-RANGING EC CHANNEL

22FOUR, THREE or TWO-POINT CALIBRATION• Proceed as described in “FIVE-POINT CALIBRATION” section.• Press ESC after the appropriate accepted calibratio

Page 16

23Wrong slopeThe calibration cannot be confirmed.The evaluated slope is less than the lowest accepted value (80% ofdefault slope).The evaluated slope

Page 17

24Wrong old slopeAn inconsistency between new and previous (old) calibration is detected.Clear old calibration parameters and initiate calibration fro

Page 18

25Use the ARROW keys to change the buffer value.Press Accept to accept new value or ESC to exit mode.Note: Custom buffer value can be adjusted within

Page 19

26The instrument will display “Calibration Cleared” and the instrumentreturns to measuring mode.ELECTRODE CONDITIONThe display is provided with an ico

Page 20

27Temperature has an effect on pH buffers. During calibration theinstrument will automatically calibrate to the pH value correspondingto the measured

Page 21

28The relative mV value calibration may be used to perform a single pointcalibration with an ORP standard or remove the contribution of thereference e

Page 22

29It is recommended to calibrate the instrument frequently, especially ifhigh accuracy is required.The ISE range should be recalibrated:• Whenever the

Page 23

3PRELIMINARY EXAMINATIONPRELIMINARY EXAMINATIONPRELIMINARY EXAMINATIONPRELIMINARY EXAMINATIONPRELIMINARY EXAMINATIONThe HI 3512 instrument is state-of

Page 24

30FIVE-POINT CALIBRATIONUse part of this procedure for 2, 3 or 4 pointcalibration. Press ESC.• Immerse the ISE electrode approximately 2 cm(¾”) into t

Page 25

31• The calibrated value and the third expected standard value will bedisplayed.• After the second calibration point is confirmed, immerse the ISEelec

Page 26

32ERROR SCREENSWrong standardThe calibration cannot be confirmed. Verify that the correct standard isselected.The message appears if mV input is out o

Page 27

33It is recommended to calibrate the instrument frequently, especially ifhigh accuracy is required.The EC range should be recalibrated:• Whenever the

Page 28 - RELATIVE RELATIVE

34• Press CAL from EC range to enter calibration mode.• Leave the probe in the air and press EC. The instrument will displaythe measured EC on the LCD

Page 29

35• When the reading is stable and close to the selected standard, theConfirm functional key is displayed.• Press Confirm to confirm calibration.ERROR

Page 30

36• Rinse the probe with some of the calibration solution or deionizedwater. Immerse the probe into HI 7037L solution. Tap the proberepeatedly to remo

Page 31

37GLP is a set of functions that allows storage and retrieval of dataregarding the maintenance and status of the electrode.All data regarding pH, Rel

Page 32

38Notes: • Buffers (standards) displayed in video inverse mode arefrom previous calibrations (pH and ISE range only).• The pH custom buffers are marke

Page 33

39LAST EC CALIBRATION DATAThe last pH calibration data is stored automatically after a successfulcalibration.To view the EC calibration data, press GL

Page 34

4• Extended temperature range on pH channel from –20 to 120 ºC(–4 to 248 ºF), using HI 7662-T interchangeable temperatureprobes.EC channel:• 7 memoriz

Page 35

40SETUPSETUPSETUPSETUPSETUPSetup mode allows viewing and modifying the measurement parameters.These are general SETUP parameters for all the ranges an

Page 36

41The following table lists the specific pH/ORP/ISE range parameters.Item Description Valid value DefaultCalibribration Number of days after Disable,

Page 37

42GENERAL PARAMETER SCREENSBacklightFocus on the Backlight item.Press Modify.Use / keys to change the intensity then press Accept to confirm.Press

Page 38 - LAST ISE CALIBRATION DATA

43Date/TimeFocus on the Date/Time item.Press Modify.Use / keys to select item.Use ARROW keys to change focused values.Press Accept to confirm new s

Page 39 - LAST NaCl % CALIBRATION DATA

44LanguageFocus on the Language item.Use the desired function key to change the option. Wait until newlanguage is loaded. If language load fails the

Page 40 - SETUPSETUP

45AutoEnd stabilityFocus on AutoEnd Stability item.Press one of the displayed function keys to select the AutoEnd stabilitycriteria.Three options are

Page 41 - Replace

46Instrument IDFocus on the Instrument ID item.Press Modify.Use ARROW keys to change the instrument ID.Press Accept to confirm or ESC to exit without

Page 42 - Contrast

47First point modeFocus on the First Point Mode item.Press the displayed function key in order to change the option.First point mode refers to the be

Page 43 - Date Format

48If Offset is set, after one point calibration the instrument evaluates theoffset and keeps the slopes unchanged.Custom BuffersFocus on the Custom Bu

Page 44 - Beep On

49View Calibration PointsFocus on the View Calibration Points item.Press the displayed function key to change option.If option is enabled the calibra

Page 45 - Log interval

51) Liquid Crystal Display (LCD)2) Function keys3) CHANNEL keys to toggle between channels (Ch1 - pH, Ch2 - EC)4) / keys to manually increase/decreas

Page 46 - Meter Information

50Focus on Charge/Slope item.Use ARROW keys in order to select the desired combination.If “None/-59.16“ is selected the slope of the probe can be cha

Page 47 - Calibration Timeout

51If Standard was pressed.Use ARROW keys to focus on the desired electrode.Press Accept to confirm setting or ESC to exit.Press View to see probe para

Page 48 - Custom Buffers

52EC CHANNEL RANGE SPECIFIC PARAMETERSCalibration TimeoutFocus on the Calibration Timeout item.Press Modify.Use ARROW keys to set desired value.Press

Page 49 - ISE probe

53Select No TC in order to display actual conductivity (no temperaturecompensation).Select MTC in order to automatically compensate conductivity using

Page 50 - Molar Weight

54Use ARROW keys to change the cell constant value.Press Accept to confirm or ESC to exit without changing.Note: If the cell constant value is modifie

Page 51 - ISE Unit

55This feature allows the user to log pH, Rel mV, ISE, EC, TDS, NaCl orResistivity measurements. All logged data can be transferred to a PCthrough the

Page 52 - T. Compensation

56Notes: • At Power Off the current lot is automatically closed.• If the 600 records space or 100 lots are reached, the “AutoLogspace is full” message

Page 53 - Cell Constant

57If Delete is pressed.Use ARROW key to focus the record to be deleted and then pressConfirm.Press ESC to exit.If Delete All is pressed the instrumet

Page 54 - Temperature Ref

58All the instruments are factory calibrated for mV, EC and temperature.Hanna’s temperature probes are interchangeable and no temperaturecalibration i

Page 55 - LOGGINGLOGGING

59• Press CAL key on the pH range or on the EC range. The calibrationscreen is displayed. Press Temp function key to enter the temperaturecalibration

Page 56 - Delete records

6Rear view10) ON/OFF switch.11) Power adaptor socket.12) USB connector.13) DIN connector for EC probe.14) BNC electrode connector for pH/ORP, ISE elec

Page 57 - Delete lot

60• Use the ARROW keys to set the calibration point value to that of thehot water.• When the reading is stable and close to the selected calibrationpo

Page 58

61Data transmission from the instrument to the PC can be done with theHI 92000 Windows® compatible software (optional). HI 92000 alsooffers graphing a

Page 59 - TEMPERATURE CALIBRATION

62CHRxx Change the instrument range according with the parametervalue (xx):• xx=10 pH range/0.001 resolution on channel 1• xx=11 pH range/0.01 resolut

Page 60

63• Resistivity, EC and temperature reading on theResistivity range• TDS, EC and temperature reading on the Resistivityrange• Salinity, EC and tempera

Page 61 - PC INTERFACE

64• The unit of the second reading (1 char) (it is sentonly for Resistivity, TDS and Salinity ranges only). Itrepresents the unit of the EC reading (0

Page 62

65• electrode condition, with sign (3 chars). The“-01” code means not calculated• ISE calibration data (if available) which contains:• the number of c

Page 63

66sign and decimal point (6 chars)• Salinity calibration data (if available), which contains:• the number of calibrated standards (1 char always 1)• t

Page 64

67encoding• 0x01 - beep ON (else OFF)• 0x02 - degrees Celsius (else Fahrenheit)• 0x04 and 0x08 - this 2 bits represent thetemperature compensation mod

Page 65

68• the log interval (5 chars): the value is in seconds; forAutoEnd log the value sent is 11000• the log starting time, yymmddhhmmss (12 chars)GLDxyqq

Page 66

69• For each record:• The number of the record (3 chars)• The reading status (1 char): R, O, U• The unit of the reading (2 chars): it is sent onlyfor

Page 67

7SPECIFICATIONSSPECIFICATIONSSPECIFICATIONSSPECIFICATIONSSPECIFICATIONSegnaRHp0.02ot0.2–Hp00.02ot00.2–Hp000.02ot000.2–Vm0.0002±.cnoc01E99.9ot7-E00.1)F

Page 68 - (not available for ISE log)

70Notes: • “Err3” is sent if the Log on demand is empty.• “Err4” is sent if the requested parameter is not available.• “Err6” is sent if the requested

Page 69

71The resistance of glass electrodes partially depends on the temperature. Thelower the temperature, the higher the resistance. It takes more time for

Page 70

72PREPARATION PROCEDURERemove the electrode protective cap.DO NOT BE ALARMED IF ANY SALT DEPOSITS ARE PRESENT. This isnormal with electrodes and they

Page 71

73For refillable electrodes:If the filling solution (electrolyte) is more than 2½ cm (1”) below the fillhole, add HI 7082 or HI 8082 3.5M KCl Electrol

Page 72

74Follow the Storage Procedure above.pH CLEANING PROCEDURE• GeneralSoak in Hanna HI 7061 or HI 8061 GeneralCleaning Solution for approximately ½ hour.

Page 73

75Rinse the probe with clean water after measurements. If more cleaningis required, remove the probe sleeve and clean the probe with a cloth ora nonab

Page 74 - Oil/grease

76TROUBLESHOOTING GUIDETROUBLESHOOTING GUIDETROUBLESHOOTING GUIDETROUBLESHOOTING GUIDETROUBLESHOOTING GUIDESMOTPMYS MELBORP NOITULOSevissecxe/esnopser

Page 75

77pH CALIBRATION SOLUTIONSHI 50004-01 pH 4.01 Buffer Solution, 20 mL sachet, 10 pcsHI 50004-02 pH 4.01 Buffer Solution, 20 mL sachet, 25 pcsHI 50007-0

Page 76 - TROUBLESHOOTING GUIDE

78120 mm4.7"12 mm0.5"5 mm0.2"3 mm0.12"3.0 mm DIA0.12"HI 1083120 mm4.7"12 mm0.5""S" VERSIONHI 1053120 mm4.

Page 77 - ACCESSORIES

7975 mm2.95"6 mm0.25""S" VERSIONHI 2031120 mm4.7"5mm0.2"5mm DIA0.2""S" VERSIONHI 1330HI 1131BGlass-body,

Page 78 - 4.7"

8CEegnaR00 mc/Sm004ot0)mc/Sm0001otpuseulavswohs(mc/Sm0001ytivitcudnoclautcAmc/Sµ999.9ot100.0mc/Sµ99.99ot00.01mc/Sµ9.999ot0.001mc/Sm999.9ot000.1mc/Sm99

Page 79 - "S" VERSION

80120 mm4.7"12 mm0.5"9.5mm DIA0.37"FC 220120 mm4.7"12 mm0.5"FC 21075 mm2.95"6 mm0.25"FC 200120 mm4.7"12 mm0.5&

Page 80 - 0.25"

81120 mm4.7"12 mm0.5"HI 4430"S" VERSION120 mm4.7"12 mm0.5"HI 3230"S" VERSION150 mm5.9"12 mm0.5""

Page 81

82EXTENSION CABLE FOR SCREW-TYPE ELECTRODES(SCREW TO BNC ADAPTER)HI 7855/1 Extension cable 1 m (3.3') longHI 7855/3 Extension cable 3 m (9.9&ap

Page 82

83RECOMMENDATIONS FOR USERSBefore using these products, make sure they are entirely suitable for theenvironment in which they are used.Operation of th

Page 83

84Printed in EUROPE(ROMANIA) MAN3512 07/10Hanna Instruments Inc.Highland Industrial Park584 Park East DriveWoonsocket, RI 02895 USATechnical Support

Page 84 - (ROMANIA) MAN3512 07/10

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